Structure of Metallo‐Supramolecular Micellar Gels
Identifieur interne : 004953 ( Main/Exploration ); précédent : 004952; suivant : 004954Structure of Metallo‐Supramolecular Micellar Gels
Auteurs : Clément Mugemana [Belgique] ; Arnaud Joset [Belgique] ; Pierre Guillet [France] ; Marie-Sousai Appavou [Allemagne] ; Nicolas De Souza [Australie] ; Charles-André Fustin [Belgique] ; Bernard Leyh [Belgique] ; Jean-François Gohy [Belgique]Source :
- Macromolecular Chemistry and Physics [ 1022-1352 ] ; 2013-08-12.
Descripteurs français
- Pascal (Inist)
- Acrylate d'alkyle copolymère, Acrylate de t-butyle copolymère, Complexation, Complexe polymère métal, Coordinat tridenté, Copolymère biséquencé, Diffusion neutron centrale, Effet concentration, Etude expérimentale, Fer II, Gel micellaire, Groupe terminal, Gélification, Ion métallique, Mécanisme, Nickel II, Polymère monodispersé, Solution alcoolique, Solution micellaire, Structure solution, Styrène copolymère, Zinc II.
- Wicri :
English descriptors
- KwdEn :
- Aggregation, Aggregation number, Alcoholic solution, Alkyl acrylate copolymer, Block copolymer, Block copolymers, Chem, Complexation, Concentration effect, Copolymer, Copolymer concentration, Core radius, Corona, Coronal, Coronal chains, Diblock copolymer, End group, Ethanol, Experimental study, Form factor, Fustin, Gelation, Gmbh, Gohy, Guillet, Gyration, Interaction distance, Intermicellar, Intermicellar chelation, Ion, Ions form, Iron II, Kgaa, Ligand, Macromol, Macromolecular chemistry, Mechanism, Metal ion, Metal ions, Micellar, Micellar network, Micellar solution, Micellar solutions, Micelle, Monodispersed polymer, Mugemana, Nagg, Neutron, Neutron science, Nickel II, Phys, Physics structure, Polymer, Ptba, Ptba chains, Ptba coronal chains, Rheology experiments, Room temperature, Sans, Sans data, Sans intensities, Small angle neutron scattering, Soft matter, Solution structure, Spatial organization, Structure factor, Structure factor peak, Styrene copolymer, Supramolecular interactions, Terpyridine, Terpyridine ligands, Total micellar radius, Total radius, Tridentate ligand, Tting procedure, Verlag, Verlag gmbh, Volume fraction, Weinheim, Wide range, Zinc II.
- Teeft :
- Aggregation, Aggregation number, Block copolymer, Block copolymers, Chem, Copolymer, Copolymer concentration, Core radius, Corona, Coronal, Coronal chains, Ethanol, Form factor, Fustin, Gmbh, Gohy, Guillet, Gyration, Interaction distance, Intermicellar, Intermicellar chelation, Ion, Ions form, Kgaa, Ligand, Macromol, Macromolecular chemistry, Metal ions, Micellar, Micellar network, Micellar solution, Micellar solutions, Micelle, Mugemana, Nagg, Neutron, Neutron science, Phys, Physics structure, Polymer, Ptba, Ptba chains, Ptba coronal chains, Rheology experiments, Room temperature, Sans, Sans data, Sans intensities, Soft matter, Spatial organization, Structure factor, Structure factor peak, Supramolecular interactions, Terpyridine, Terpyridine ligands, Total micellar radius, Total radius, Tting procedure, Verlag, Verlag gmbh, Volume fraction, Weinheim, Wide range.
Abstract
A small‐angle neutron scattering investigation of metallo‐supramolecular micellar gels built from polystyrene‐block‐poly(tert‐butylacrylate) PS‐b‐PtBA‐tpy (‐tpy: terpyridine) block copolymers and transition metal ions is presented. The influence of the copolymer concentration on the structure and spatial organization of the micelles, as well as the impact of the subsequent addition of metal ions (Fe(II), Ni(II), and Zn(II)) on these characteristics is extensively studied. The experimental scattering cross‐sections are fitted with an analytical formula based on the Percus–Yevick hard‐sphere model and on the Pedersen–Gerstenberg model for the structure and the form factor, respectively. The resulting structural information is correlated with previously performed light scattering and rheology experiments.
Url:
DOI: 10.1002/macp.201300288
Affiliations:
- Allemagne, Australie, Belgique, France
- Provence-Alpes-Côte d'Azur, Province de Liège, Région wallonne, Vienne (Autriche)
- Avignon, Liège, Louvain-la-Neuve, Vienne (Autriche)
- Université catholique de Louvain, Université d'Avignon, Université de Liège
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Le document en format XML
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first="Clément" last="Mugemana">Clément Mugemana</name><affiliation wicri:level="4"><country xml:lang="fr">Belgique</country><wicri:regionArea>Université Catholique de Louvain, Institute of Condensed Matter and Nanosciences (IMCN), Bio‐ and Soft Matter division (BSMA), Place Pasteur 1, 1348 Louvain‐la‐Neuve</wicri:regionArea><placeName><region type="land" nuts="2">Vienne (Autriche)</region><settlement type="city">Vienne (Autriche)</settlement><settlement type="city">Louvain-la-Neuve</settlement></placeName><orgName type="university">Université catholique de Louvain</orgName></affiliation></author><author><name sortKey="Joset, Arnaud" sort="Joset, Arnaud" uniqKey="Joset A" first="Arnaud" last="Joset">Arnaud Joset</name><affiliation wicri:level="4"><country xml:lang="fr">Belgique</country><wicri:regionArea>University of Liège, Department of Chemistry, Molecular Dynamics Laboratory, B‐4000 Sart‐Tilman</wicri:regionArea><orgName type="university">Université de Liège</orgName><placeName><settlement type="city">Liège</settlement><region type="region" nuts="1">Région wallonne</region><region type="province" nuts="1">Province de Liège</region></placeName></affiliation></author><author><name sortKey="Guillet, Pierre" sort="Guillet, Pierre" uniqKey="Guillet P" first="Pierre" last="Guillet">Pierre Guillet</name><affiliation wicri:level="4"><country xml:lang="fr">France</country><wicri:regionArea>Université d'Avignon et des Pays de Vaucluse, Equipe Chimie Bioorganique et Systèmes Amphiphiles, 84000 Avignon</wicri:regionArea><placeName><region type="region" nuts="2">Provence-Alpes-Côte d'Azur</region><settlement type="city">Avignon</settlement><settlement type="city">Avignon</settlement></placeName><orgName type="university">Université d'Avignon</orgName></affiliation></author><author><name sortKey="Appavou, Marie Ousai" sort="Appavou, Marie Ousai" uniqKey="Appavou M" first="Marie-Sousai" last="Appavou">Marie-Sousai Appavou</name><affiliation wicri:level="1"><country xml:lang="fr">Allemagne</country><wicri:regionArea>Forschungszentrum Jülich GmbH, Jülich Centre for Neutron Science at FRM II, Lichtenbergstr. 1, 85747 Garching</wicri:regionArea><wicri:noRegion>85747 Garching</wicri:noRegion><wicri:noRegion>85747 Garching</wicri:noRegion></affiliation></author><author><name sortKey="De Souza, Nicolas" sort="De Souza, Nicolas" uniqKey="De Souza N" first="Nicolas" last="De Souza">Nicolas De Souza</name><affiliation wicri:level="1"><country xml:lang="fr">Australie</country><wicri:regionArea>Bragg Institute, Australian Nuclear Science and Technology Organisation Locked Bag 2001, Kirrawee DC NSW 223</wicri:regionArea><wicri:noRegion>Kirrawee DC NSW 223</wicri:noRegion></affiliation></author><author><name sortKey="Fustin, Charles Ndre" sort="Fustin, Charles Ndre" uniqKey="Fustin C" first="Charles-André" last="Fustin">Charles-André Fustin</name><affiliation wicri:level="4"><country xml:lang="fr">Belgique</country><wicri:regionArea>Université Catholique de Louvain, Institute of Condensed Matter and Nanosciences (IMCN), Bio‐ and Soft Matter division (BSMA), Place Pasteur 1, 1348 Louvain‐la‐Neuve</wicri:regionArea><placeName><region type="land" nuts="2">Vienne (Autriche)</region><settlement type="city">Vienne (Autriche)</settlement><settlement type="city">Louvain-la-Neuve</settlement></placeName><orgName type="university">Université catholique de Louvain</orgName></affiliation><affiliation wicri:level="1"><country wicri:rule="url">Belgique</country></affiliation><affiliation wicri:level="4"><country xml:lang="fr">Belgique</country><wicri:regionArea>Charles‐André Fustin, Université Catholique de Louvain, Institute of Condensed Matter and Nanosciences (IMCN), Bio‐ and Soft Matter division (BSMA), Place Pasteur 1, 1348 Louvain‐la‐Neuve, BelgiumBernard Leyh, University of Liège, Department of Chemistry, Molecular Dynamics Laboratory, B‐4000 Sart‐Tilman, Belgium.Jean‐François Gohy, Université Catholique de Louvain, Institute of Condensed Matter and Nanosciences (IMCN), Bio‐ and Soft Matter division (BSMA), Place Pasteur 1, 1348 Louvain‐la‐Neuve</wicri:regionArea><placeName><region type="land" nuts="2">Vienne (Autriche)</region><settlement type="city">Vienne (Autriche)</settlement><settlement type="city">Louvain-la-Neuve</settlement></placeName><orgName type="university">Université catholique de Louvain</orgName></affiliation></author><author><name sortKey="Leyh, Bernard" sort="Leyh, Bernard" uniqKey="Leyh B" first="Bernard" last="Leyh">Bernard Leyh</name><affiliation wicri:level="4"><country xml:lang="fr">Belgique</country><wicri:regionArea>University of Liège, Department of Chemistry, Molecular Dynamics Laboratory, B‐4000 Sart‐Tilman</wicri:regionArea><orgName type="university">Université de Liège</orgName><placeName><settlement type="city">Liège</settlement><region type="region" nuts="1">Région wallonne</region><region type="province" nuts="1">Province de Liège</region></placeName></affiliation><affiliation wicri:level="1"><country wicri:rule="url">Belgique</country></affiliation><affiliation wicri:level="4"><country xml:lang="fr">Belgique</country><wicri:regionArea>Charles‐André Fustin, Université Catholique de Louvain, Institute of Condensed Matter and Nanosciences (IMCN), Bio‐ and Soft Matter division (BSMA), Place Pasteur 1, 1348 Louvain‐la‐Neuve, BelgiumBernard Leyh, University of Liège, Department of Chemistry, Molecular Dynamics Laboratory, B‐4000 Sart‐Tilman, Belgium.Jean‐François Gohy, Université Catholique de Louvain, Institute of Condensed Matter and Nanosciences (IMCN), Bio‐ and Soft Matter division (BSMA), Place Pasteur 1, 1348 Louvain‐la‐Neuve</wicri:regionArea><placeName><region type="land" nuts="2">Vienne (Autriche)</region><settlement type="city">Vienne (Autriche)</settlement><settlement type="city">Louvain-la-Neuve</settlement></placeName><orgName type="university">Université catholique de Louvain</orgName></affiliation></author><author><name sortKey="Gohy, Jean Rancois" sort="Gohy, Jean Rancois" uniqKey="Gohy J" first="Jean-François" last="Gohy">Jean-François Gohy</name><affiliation wicri:level="4"><country xml:lang="fr">Belgique</country><wicri:regionArea>Université Catholique de Louvain, Institute of Condensed Matter and Nanosciences (IMCN), Bio‐ and Soft Matter division (BSMA), Place Pasteur 1, 1348 Louvain‐la‐Neuve</wicri:regionArea><placeName><region type="land" nuts="2">Vienne (Autriche)</region><settlement type="city">Vienne (Autriche)</settlement><settlement type="city">Louvain-la-Neuve</settlement></placeName><orgName type="university">Université catholique de Louvain</orgName></affiliation><affiliation wicri:level="1"><country wicri:rule="url">Belgique</country></affiliation><affiliation wicri:level="4"><country xml:lang="fr">Belgique</country><wicri:regionArea>Charles‐André Fustin, Université Catholique de Louvain, Institute of Condensed Matter and Nanosciences (IMCN), Bio‐ and Soft Matter division (BSMA), Place Pasteur 1, 1348 Louvain‐la‐Neuve, BelgiumBernard Leyh, University of Liège, Department of Chemistry, Molecular Dynamics Laboratory, B‐4000 Sart‐Tilman, Belgium.Jean‐François Gohy, Université Catholique de Louvain, Institute of Condensed Matter and Nanosciences (IMCN), Bio‐ and Soft Matter division (BSMA), Place Pasteur 1, 1348 Louvain‐la‐Neuve</wicri:regionArea><placeName><region type="land" nuts="2">Vienne (Autriche)</region><settlement type="city">Vienne (Autriche)</settlement><settlement type="city">Louvain-la-Neuve</settlement></placeName><orgName type="university">Université catholique de Louvain</orgName></affiliation></author></analytic><monogr></monogr><series><title level="j" type="main">Macromolecular Chemistry and Physics</title><title level="j" type="alt">MACROMOLECULAR CHEMISTRY AND PHYSICS</title><idno type="ISSN">1022-1352</idno><idno type="eISSN">1521-3935</idno><imprint><biblScope unit="vol">214</biblScope><biblScope unit="issue">15</biblScope><biblScope unit="page" from="1699">1699</biblScope><biblScope unit="page" to="1709">1709</biblScope><biblScope unit="page-count">11</biblScope><publisher>WILEY‐VCH Verlag</publisher><pubPlace>Weinheim</pubPlace><date type="published" when="2013-08-12">2013-08-12</date></imprint><idno type="ISSN">1022-1352</idno></series></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">1022-1352</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Aggregation</term><term>Aggregation number</term><term>Alcoholic solution</term><term>Alkyl acrylate copolymer</term><term>Block copolymer</term><term>Block copolymers</term><term>Chem</term><term>Complexation</term><term>Concentration effect</term><term>Copolymer</term><term>Copolymer concentration</term><term>Core radius</term><term>Corona</term><term>Coronal</term><term>Coronal chains</term><term>Diblock copolymer</term><term>End group</term><term>Ethanol</term><term>Experimental study</term><term>Form factor</term><term>Fustin</term><term>Gelation</term><term>Gmbh</term><term>Gohy</term><term>Guillet</term><term>Gyration</term><term>Interaction distance</term><term>Intermicellar</term><term>Intermicellar chelation</term><term>Ion</term><term>Ions form</term><term>Iron II</term><term>Kgaa</term><term>Ligand</term><term>Macromol</term><term>Macromolecular chemistry</term><term>Mechanism</term><term>Metal ion</term><term>Metal ions</term><term>Micellar</term><term>Micellar network</term><term>Micellar solution</term><term>Micellar solutions</term><term>Micelle</term><term>Monodispersed polymer</term><term>Mugemana</term><term>Nagg</term><term>Neutron</term><term>Neutron science</term><term>Nickel II</term><term>Phys</term><term>Physics structure</term><term>Polymer</term><term>Ptba</term><term>Ptba chains</term><term>Ptba coronal chains</term><term>Rheology experiments</term><term>Room temperature</term><term>Sans</term><term>Sans data</term><term>Sans intensities</term><term>Small angle neutron scattering</term><term>Soft matter</term><term>Solution structure</term><term>Spatial organization</term><term>Structure factor</term><term>Structure factor peak</term><term>Styrene copolymer</term><term>Supramolecular interactions</term><term>Terpyridine</term><term>Terpyridine ligands</term><term>Total micellar radius</term><term>Total radius</term><term>Tridentate ligand</term><term>Tting procedure</term><term>Verlag</term><term>Verlag gmbh</term><term>Volume fraction</term><term>Weinheim</term><term>Wide range</term><term>Zinc II</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Acrylate d'alkyle copolymère</term><term>Acrylate de t-butyle copolymère</term><term>Complexation</term><term>Complexe polymère métal</term><term>Coordinat tridenté</term><term>Copolymère biséquencé</term><term>Diffusion neutron centrale</term><term>Effet concentration</term><term>Etude expérimentale</term><term>Fer II</term><term>Gel micellaire</term><term>Groupe terminal</term><term>Gélification</term><term>Ion métallique</term><term>Mécanisme</term><term>Nickel II</term><term>Polymère monodispersé</term><term>Solution alcoolique</term><term>Solution micellaire</term><term>Structure solution</term><term>Styrène copolymère</term><term>Zinc II</term></keywords><keywords scheme="Teeft" xml:lang="en"><term>Aggregation</term><term>Aggregation number</term><term>Block copolymer</term><term>Block copolymers</term><term>Chem</term><term>Copolymer</term><term>Copolymer concentration</term><term>Core radius</term><term>Corona</term><term>Coronal</term><term>Coronal chains</term><term>Ethanol</term><term>Form factor</term><term>Fustin</term><term>Gmbh</term><term>Gohy</term><term>Guillet</term><term>Gyration</term><term>Interaction distance</term><term>Intermicellar</term><term>Intermicellar chelation</term><term>Ion</term><term>Ions form</term><term>Kgaa</term><term>Ligand</term><term>Macromol</term><term>Macromolecular chemistry</term><term>Metal ions</term><term>Micellar</term><term>Micellar network</term><term>Micellar solution</term><term>Micellar solutions</term><term>Micelle</term><term>Mugemana</term><term>Nagg</term><term>Neutron</term><term>Neutron science</term><term>Phys</term><term>Physics structure</term><term>Polymer</term><term>Ptba</term><term>Ptba chains</term><term>Ptba coronal chains</term><term>Rheology experiments</term><term>Room temperature</term><term>Sans</term><term>Sans data</term><term>Sans intensities</term><term>Soft matter</term><term>Spatial organization</term><term>Structure factor</term><term>Structure factor peak</term><term>Supramolecular interactions</term><term>Terpyridine</term><term>Terpyridine ligands</term><term>Total micellar radius</term><term>Total radius</term><term>Tting procedure</term><term>Verlag</term><term>Verlag gmbh</term><term>Volume fraction</term><term>Weinheim</term><term>Wide range</term></keywords><keywords scheme="Wicri" type="topic" xml:lang="fr"><term>éthanol</term><term>Polymère</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">A small‐angle neutron scattering investigation of metallo‐supramolecular micellar gels built from polystyrene‐block‐poly(tert‐butylacrylate) PS‐b‐PtBA‐tpy (‐tpy: terpyridine) block copolymers and transition metal ions is presented. The influence of the copolymer concentration on the structure and spatial organization of the micelles, as well as the impact of the subsequent addition of metal ions (Fe(II), Ni(II), and Zn(II)) on these characteristics is extensively studied. The experimental scattering cross‐sections are fitted with an analytical formula based on the Percus–Yevick hard‐sphere model and on the Pedersen–Gerstenberg model for the structure and the form factor, respectively. The resulting structural information is correlated with previously performed light scattering and rheology experiments.</div></front></TEI><affiliations><list><country><li>Allemagne</li><li>Australie</li><li>Belgique</li><li>France</li></country><region><li>Provence-Alpes-Côte d'Azur</li><li>Province de Liège</li><li>Région wallonne</li><li>Vienne (Autriche)</li></region><settlement><li>Avignon</li><li>Liège</li><li>Louvain-la-Neuve</li><li>Vienne (Autriche)</li></settlement><orgName><li>Université catholique de Louvain</li><li>Université d'Avignon</li><li>Université de Liège</li></orgName></list><tree><country name="Belgique"><region name="Vienne (Autriche)"><name sortKey="Mugemana, Clement" sort="Mugemana, Clement" uniqKey="Mugemana C" first="Clément" last="Mugemana">Clément Mugemana</name></region><name sortKey="Fustin, Charles Ndre" sort="Fustin, Charles Ndre" uniqKey="Fustin C" first="Charles-André" last="Fustin">Charles-André Fustin</name><name sortKey="Fustin, Charles Ndre" sort="Fustin, Charles Ndre" uniqKey="Fustin C" first="Charles-André" last="Fustin">Charles-André Fustin</name><name sortKey="Fustin, Charles Ndre" sort="Fustin, Charles Ndre" uniqKey="Fustin C" first="Charles-André" last="Fustin">Charles-André Fustin</name><name sortKey="Gohy, Jean Rancois" sort="Gohy, Jean Rancois" uniqKey="Gohy J" first="Jean-François" last="Gohy">Jean-François Gohy</name><name sortKey="Gohy, Jean Rancois" sort="Gohy, Jean Rancois" uniqKey="Gohy J" first="Jean-François" last="Gohy">Jean-François Gohy</name><name sortKey="Gohy, Jean Rancois" sort="Gohy, Jean Rancois" uniqKey="Gohy J" first="Jean-François" last="Gohy">Jean-François Gohy</name><name sortKey="Joset, Arnaud" sort="Joset, Arnaud" uniqKey="Joset A" first="Arnaud" last="Joset">Arnaud Joset</name><name sortKey="Leyh, Bernard" sort="Leyh, Bernard" uniqKey="Leyh B" first="Bernard" last="Leyh">Bernard Leyh</name><name sortKey="Leyh, Bernard" sort="Leyh, Bernard" uniqKey="Leyh B" first="Bernard" last="Leyh">Bernard Leyh</name><name sortKey="Leyh, Bernard" sort="Leyh, Bernard" uniqKey="Leyh B" first="Bernard" last="Leyh">Bernard Leyh</name></country><country name="France"><region name="Provence-Alpes-Côte d'Azur"><name sortKey="Guillet, Pierre" sort="Guillet, Pierre" uniqKey="Guillet P" first="Pierre" last="Guillet">Pierre Guillet</name></region></country><country name="Allemagne"><noRegion><name sortKey="Appavou, Marie Ousai" sort="Appavou, Marie Ousai" uniqKey="Appavou M" first="Marie-Sousai" last="Appavou">Marie-Sousai Appavou</name></noRegion></country><country name="Australie"><noRegion><name sortKey="De Souza, Nicolas" sort="De Souza, Nicolas" uniqKey="De Souza N" first="Nicolas" last="De Souza">Nicolas De Souza</name></noRegion></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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